Preparation of Sulphonated Zirconium Phosphate-Phenylphosphonates and Their Catalytic Properties in Carbonylation of Formaldehyde

Chinese Journal of Catalysis ›› 2009, Vol. 30 ›› Issue (8): 786-790.

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Preparation of Sulphonated Zirconium Phosphate-Phenylphosphonates and Their Catalytic Properties in Carbonylation of Formaldehyde

SUN Ying1, 2, ZHANG Yangyang1, QI Yue1, WANG Hua1, LIU Hongchao1, SHEN Jianghan1, LIU Zhong-min1,*

1Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, Liaoning, China 2Graduate University of Chinese Academy of Sciences, Beijing 100049, China

Received:2009-08-25 Online:2009-08-25 Published:2013-05-16

Abstract

Abstract: A series of zirconium phosphate sulfophenylphosphonates (SZrPP-n) were synthesized and characterized. SZrPP-n possessed a high acidity amount and thermal stability with layered structure. As a solid acid catalyst, SZrPP-n exhibited high catalytic activity and stability for methyl glycolate synthesis from carbonylation of HCHO with CO under mild conditions.

Key words: zirconium phenyl phosphonate, sulfonation, formaldehyde, carbonylation, methyl glycolate

SUN Ying;;ZHANG Yangyang;QI Yue;WANG Hua;LIU Hongchao;SHEN Jianghan;LIU Zhong-min;*. Preparation of Sulphonated Zirconium Phosphate-Phenylphosphonates and Their Catalytic Properties in Carbonylation of Formaldehyde[J]. Chinese Journal of Catalysis, 2009, 30(8): 786-790.

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Preparation of Sulphonated Zirconium Phosphate-Phenylphosphonates and Their Catalytic Properties in Carbonylation of Formaldehyde

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