In-situ Electrochemical Characterization Methodology

Abstract

Abstract: With increasing demand of clean energy, electrochemical energy storage technologies have attracted intensive research interest. In-situ electrochemical characterization with high temporal and spatial resolutions has become increasingly important for investigation of the electrochemical processes in close-to-real electrochemical energy storage devices. This paper reviews the progress of in-situ electrochemical characterization methodology, including in-situ transmission electron microscopy, synchrotron radiation X-ray spectroscopy, and sum frequency generation spectroscopy. The challenges facing in-situ electrochemical characterization and the prospects for further methodological development are presented.

Key words: electrochemistry, energy storage, in-situ characterization, transmission electron microscopy, synchrotron radiation, X-ray absorption spectroscopy, sum frequency generation spectroscopy

XU Guoguang, WANG Min, WANG Jian, LIN Hongzhen, WU Yang, WEI Yang, ZHANG Yuegang. In-situ Electrochemical Characterization Methodology[J]. Chinese Journal of Catalysis, 2019, 40(s1): 187-199.

×
share this article

Add to citation manager EndNote|Ris|BibTeX

URL: https://www.cjcatal.com/EN/

https://www.cjcatal.com/EN/Y2019/V40/Is1/187

References

1 Goodenough J B, Kim Y. Chem Mater, 2010, 22:587
2 Dunn B, Kamath H, Tarascon J M. Science, 2011, 334:928
3 Liu X H, Huang J Y. Energy Environ Sci, 2011, 4:3844
4 Xu F, Wu L, Meng Q, Kaltak M, Huang J, Durham J L, Fernandez-Serra M, Sun L, Marschilok A C, Takeuchi E S, Takeuchi K J, Hybertsen M S, Zhu Y. Nat Commun, 2017, 8:15400
5 Wang L, Xu Z, Wang W, Bai X. J Am Chem Soc, 2014, 136:6693
6 Liang W, Yang H, Fan F, Liu Y, Liu X H, Huang J Y, Zhu T, Zhang S. ACS Nano, 2013, 7:3427
7 Janish M T, Mackay D T, Liu Y, Jungjohann K L, Carter C B, Norton M G. J Mater Sci, 2016, 51:589
8 Huang J Y, Zhong L, Wang C M, Sullivan J P, Xu W, Zhang L Q, Mao S X, Hudak N S, Liu X H, Subramanian A, Fan H, Qi L, Kushima A, Li J. Science, 2010, 330:1515
9 Zhang L Q, Liu X H, Liu Y, Huang S, Zhu T, Gui L, Mao S X, Ye Z Z, Chong M, Sullivan J P, Huang J Y. ACS Nano, 2011, 5:4800
10 Gong Y, Zhang J, Jiang L, Shi J A, Zhang Q, Yang Z, Zou D, Wang J, Yu X, Xiao R, Hu Y S, Gu L, Li H, Chen L. J Am Chem Soc, 2017, 139:4274
11 Li N W, Yin Y X, Yang C P, Guo Y G. Adv Mater, 2016, 28:1853
12 Zeng Z, Liang W I, Liao H G, Xin H L, Chu Y H, Zheng H. Nano Lett, 2014, 14:1745
13 Rong G, Zhang X, Zhao W, Qiu Y, Liu M, Ye F, Xu Y, Chen J, Hou Y, Li W, Duan W, Zhang Y. Adv Mater, 2017, 29:1606187
14 Ohta N, Takada K, Zhang L, Ma R, Osada M, Sasaki T. Adv Mater, 2006, 18:2226
15 Sakuda A, Hayashi A, Tatsumisago M. Chem Mater, 2010, 3:949
16 Sakuda A, Hayashi A, Ohtomo T, Hama S, Tatsumisago M. Electrochem Solid State Lett, 2010, 13:A73
17 Yamamoto K, Yoshida R, Sato T, Matsumoto H, Kurobe H, Hamanaka T, Kato T, Iriyama Y, Hirayama T. J Power Sources, 2014, 266:414
18 Yamamoto K, Iriyama Y, Hirayama T. Microscopy, 2017, 66:50
19 Liu X H, Zhang L Q, Zhong L, Liu Y, Zheng H, Wang J W, Cho J H, Dayeh S A, Picraux S T, Sullivan J P, Mao S X, Ye Z Z, Huang J Y. Nano Lett, 2011, 11:2251
20 McDowell M T, Ryu I, Lee S W, Wang C, Nix W D, Cui Y. Adv Mater, 2012, 24:6034
21 Gu M, Yang H, Perea D E, Zhang J G, Zhang S, Wang C M. Nano Lett, 2014, 14:4622
22 Zhu Y, Wang J W, Liu Y, Liu X, Kushima A, Liu Y, Xu Y, Mao S X, Li J, Wang C, Huang J Y. Adv Mater, 2013, 25:5461
23 Northrup P, Leri A, Tappero R. Protein Pept Lett, 2016, 23:300
24 Yano J, Yachandra V K. Photosynth Res, 2009, 102:241
25 Tsai Y, Lee J, Liu D, Hwang B. J Mater Chem, 2004, 14:958
26 Brownrigg A W, Mountjoy G, Chadwick A V, Alfredsson M, Bras W, Billaud J, Armstrong A R, Bruce P G, Dominko R, Kelder E M. J Mater Chem A, 2015, 3:7314
27 Terada Y, Yasaka K, Nishikawa F, Konishi T, Yoshio M, Nakai I. J Solid State Chem, 2001, 156:286
28 Katayama M, Sumiwaka K, Miyahara R, Yamashige H, Arai H, Uchimoto Y, Ohta T, Inada Y, Ogumi Z. J Power Sources, 2014, 269:994
29 Liu X, Liu J, Qiao R, Yu Y, Li H, Suo L, Hu Y, Chuang Y, Shu G, Chou F, Weng T C, Nordlund D, Sokaras D, Wang Y J, Lin H, Barbiellini B, Bansil A, Song X, Liu Z, Yan S, Liu G, Qiao S, Richardson T J, Prendergast D, Hussain Z, Frank M. F. de Groot, Yang W. J Am Chem Soc, 2012, 134:13708.
30 Balasubramanian M, Sun X, Yang X, McBreen J. J Electrochem Soc, 2000, 147:2903
31 Nonaka T, Okuda C, Seno Y, Nakano Y, Koumoto K, Ukyo Y. J Power Sources, 2006, 162:1329
32 Yoon W S, Grey C P, Balasubramanian M, Yang X Q, McBreen J. Chem Mater, 2003, 15:3161
33 Yoon W S, Balasubramanian M, Chung K Y,Yang X Q, McBreen J, Grey C P, Fischer D A. J Am Chem Soc, 2005, 127:17479
34 Tsai Y, Hwang B, Ceder G, Sheu H, Liu D, Lee J. Chem Mater, 2005, 17:3191
35 Yu X, Lyu Y, Gu L, Wu H, Bak S M, Zhou Y, Amine K, Ehrlich S N, Li H, Nam K W. Adv Energy Mater, 2014, 4:1300950
36 Colbow K, Dahn J, Haering R. J Power Sources, 1989, 26:397
37 Ohzuku T, Ueda A, Yamamoto N. J Electrochem Soc, 1995, 142:1431
38 Scharner S, Weppner W, Schmid-Beurmann P. J Electrochem Soc, 1999, 146:857
39 Wagemaker M, Simon D R, Kelder E M, Schoonman J, Ringpfeil C, Haake U, Lützenkirchen-Hecht D, Frahm R, Mulder F M. Adv Mater, 2006, 18:3169
40 Kim S, Fang S, Zhang Z, Chen J, Yang L, Penner-Hahn J E, Deb A. J Power Sources, 2014, 268:294
41 Venkateswarlu M, Chen C, Do J, Lin C, Chou T C, Hwang B. J Power Sources, 2005, 146:204
42 Zhang W, Topsakal M, Cama C, Pelliccione C J, Zhao H, Ehrlich S, Wu L, Zhu Y, Frenkel A I, Takeuchi K J, Takeuchi E S, Marschilok A C, Lu D, Wang F. J Am Chem Soc, 2017, 139:16591
43 Nam K W, Bak S M, Hu E Y, Yu X Q, Zhou Y N, Wang X J, Wu L J, Zhu Y M, Chung K Y, Yang X Q. Ad. Funct Mater, 2013, 23:1047
44 Hu E, Bak S M, Liu J, Yu X, Zhou Y, Ehrlich S N, Yang X Q, Nam K W. Chem Mater, 2014, 26:11108
45 Yin Y X, Xin S, Guo Y G, Wan L J, Angew Chem Int Ed, 2013, 52:13186
46 Manthiram A, Fu Y, Chung S H, Zu C, Su Y S. Chem Rev, 2014, 114:11751
47 Manthiram A, Fu Y, Su Y S. Acc Chem Res, 2012, 46:1125
48 Cuisinier M, Cabelguen P E, Evers S, He G, Kolbeck M, Garsuch A, Bolin T, Balasubramanian M, Nazar L F. J Phys Chem Lett, 2013, 4:3227
49 Zhang L, Sun D, Feng J, Cairns E J, Guo J. Nano Lett, 2017, 17:5084
50 Zhang L, Ling M, Feng J, Liu G, Guo J. Nano Energy, 2017, 40:559
51 Ling M, Zhang L, Zheng T, Feng J, Guo J, Mai L, Liu G. Nano Energy, 2017, 38:82
52 Yoo H D, Liang Y, Dong H, Lin J, Wang H, Liu Y, Ma L, Wu T, Li Y, Ru Q, Jing Y, An Q, Zhou W, Guo J, Lu J, Pantelides S T, Qian X, Yao Y. Nat Commun, 2017, 8:339
53 Koketsu T, Ma J, Morgan B J, Body M, Legein C, Dachraoui W, Giannini M, Demortière A, Salanne M, Dardoize F, Groult H, Borkiewicz O J, Chapman K W, Strasser P, Dambournet D. Nat Mater, 2017, 16:1142
54 Kim H S, Arthur T S, Allred G D, Zajicek J, Newman J G, Rodnyansky A E, Oliver A G, Boggess W C, Muldoon J. Nat Commun, 2011, 2:427
55 Yu X, Manthiram A. ACS Energy Lett, 2016, 1:431
56 Vinayan B P, Zhao-Karger Z, Diemant T, Chakravadhanula V S K, Schwarzburger N I, Cambaz M A, Behm R J, Kubel C, Fichtner M. Nanoscale, 2016, 8:3296
57 Xu Y, Ye Y, Zhao S, Feng J, Li J, Chen H, Yang A, Shi F, Jia L, Wu Y, Yu X, Per-Anders Glans-Suzuki, Cui Y, Guo J, Zhang Y. Nano Lett, 2019, 19:2928
58 Nelson J, Misra S, Yang Y, Jackson A, Liu Y, Wang H, Dai H, Andrews J C, Cui Y, Toney M F. J Am Chem Soc, 2012, 134:6337
59 Weker J N, Liu N, Misra S, Andrews J C, Cui Y, Toney M F. Energy Environ Sci, 2014, 7:2771
60 Chao S C, Yen Y C, Song Y F, Sheu H S, Wu H C, Wu N L. J Electrochem Soc, 2011, 158:A1335
61 Boesenberg U, Meirer F, Liu Y, Shukla A K, Anna D R, Ty-liszczak T, Chen G, Andrews J C, Richardson T J, Kostecki R. Chem Mater, 2013, 25:1664
62 Yang F F, Liu Y, Martha S K, Wu Z, Andrews J C, Ice G E, Pianetta P, Nanda J. Nano Lett, 2014, 14:4334
63 Lin F, Nordlund D, Li Y, Quan M K, Cheng L, Weng T C, Liu Y, Xin H, Doeff M M. Nat Energy, 2016, 1:15004
64 de Smit E, Swart I, Creemer J F, Hoveling G H, Gilles M K, Tyliszczak T, Kooyman P J, Zandbergen H W, Morin C, Weckhuysen B M, de Groot F M F. Nature, 2008, 456:222
65 Lim J, Li Y, Alsem D H, So H, Lee S C, Bai P, Cogswell D A, Liu X, Jin N, Yu Y S, Salmon N J, Shapiro D A, Bazant M Z, Tyliszczak T, Chueh W C. Science, 2016, 353:566
66 Yu L, Liu H J, Wang Y,Kuwata N, Osawa M, Kawamura J, Ye S. Angew Chem Int Ed, 2013, 52:5753
67 (a) Mukherjee P, Lagutchev A, Dlott D D. J Electrochem Soc, 2012, 159:A244; (b) Nicolau B G, Garcia-Rey N, Dryzhakov B, Dlott D D. J. Phys. Chem. C, 2015, 119:10227
68 Horowitz Y, Han H L, Ross P N, Somorjai G A. J Am Chem Soc, 2016, 138:726
69 Horowitz Y, Steinrück H G, Han H L, Cao C, Abate I I, Tsao Y, Toney M F, Somorjai G A. Nano Lett, 2018, 18:2105
70 (a) Horowitz Y, Han H L, Ralston W T, de Araujo J R, Kreidler E, Brooks C, Somorjai G A. Adv Energy Mater, 2017, 7:1602060; (b) Horowitz Y, Han H L, Soto F A, Ralston W T, Balbuena P B, Somorjai G A. Nano Lett, 2018, 18:1145
71 Olson J Z, Johansson P K, Castner D G, Schlenker C W. Chem Mater, 2018, 30:1239
72 Kang T, Wang Y, Guo F, Liu C, Zhao J, Yang J, Lin H, Qiu Y, Shen Y, Lu W, Chen L. ACS Central Sci, 2019, 5:468
73 Peng Q, Chen J, Ji H, Morita A, Ye S. J Am Chem Soc, 2018, 140:15568
74 Neri G, Walsh J J, Teobaldi G, Donaldson P M, Cowan A J. Nat Catal, 2018, 1:952
75 Howie A. J Microscopy, 1979, 116:89
76 Leenheer A J, Jungjohann K L, Zavadil K R, Harris C T. ACS Nano, 2016, 6:5670

[1]	Liqun Wang, Xiao Yan, Wenping Si, Daolan Liu, Xinggang Hou, Dejun Li, Feng Hou, Shi Xue Dou, Ji Liang. Photoelectrochemical nitrogen reduction: A step toward achieving sustainable ammonia synthesis [J]. Chinese Journal of Catalysis, 2022, 43(7): 1761-1773.
[2]	Heng-Quan Chen, Lie Zou, Di-Ye Wei, Ling-Ling Zheng, Yuan-Fei Wu, Hua Zhang, Jian-Feng Li. In situ studies of energy-related electrochemical reactions using Raman and X-ray absorption spectroscopy [J]. Chinese Journal of Catalysis, 2022, 43(1): 33-46.
[3]	Jin-Yang Chen, Hong-Yu Wu, Qing-Wen Gui, Shan-Shu Yan, Jie Deng, Ying-Wu Lin, Zhong Cao, Wei-Min He. Sustainable electrochemical cross-dehydrogenative coupling of 4-quinolones and diorganyl diselenides [J]. Chinese Journal of Catalysis, 2021, 42(9): 1445-1450.
[4]	Chenxin Yang, Henan Chen, Tao Peng, Baiyao Liang, Yun Zhang, Wei Zhao. Lignin valorization toward value-added chemicals and fuels via electrocatalysis: A perspective [J]. Chinese Journal of Catalysis, 2021, 42(11): 1831-1842.
[5]	Yaroslava Lykhach, Tomá? Skála, Armin Neitzel, Nataliya Tsud, Klára Beranová, Kevin C. Prince, Vladimír Matolín, J?rg Libuda. Nanoscale architecture of ceria-based model catalysts: Pt-Co nanostructures on well-ordered CeO₂(111) thin films [J]. Chinese Journal of Catalysis, 2020, 41(6): 985-997.
[6]	FANG Yahui, LIU Zhipan. Insight into the Important Electrochemical Reactions from First-Principles Calcualtions [J]. Chinese Journal of Catalysis, 2019, 40(s1): 90-97.
[7]	XIA Lan, CHEN Z. George. High Density Electrochemical Energy Storage via Regenerative Fuels [J]. Chinese Journal of Catalysis, 2019, 40(s1): 111-119.
[8]	HAN Yong, ZHANG Hui, LIU Zhi. Ambient-Pressure X-ray Photoelectron Spectroscopy in Catalysis [J]. Chinese Journal of Catalysis, 2019, 40(s1): 200-208.
[9]	Erwin Lam, Kim Larmier, Shohei Tada, Patrick Wolf, Olga V. Safonova, Christophe Copéret. Zr(IV) surface sites determine CH₃OH formation rate on Cu/ZrO₂/SiO₂-CO₂ hydrogenation catalysts [J]. Chinese Journal of Catalysis, 2019, 40(11): 1741-1748.
[10]	Jiansheng Li, Lei Wang, Wansheng You, Meiying Liu, Lancui Zhang, Xiaojing Sang. Catalytic effects of[Ag(H₂O)(H₃PW₁₁O₃₉)]^3- on a TiO₂ anode for water oxidation [J]. Chinese Journal of Catalysis, 2018, 39(3): 534-541.
[11]	Xiaobo He, Fengxiang Yin, Hao Wang, Biaohua Chen, Guoru Li. Metal-organic frameworks for highly efficient oxygen electrocatalysis [J]. Chinese Journal of Catalysis, 2018, 39(2): 207-227.
[12]	Guangxian Pei, Xiaoyan Liu, Mengqian Chai, Aiqin Wang, Tao Zhang. Isolation of Pd atoms by Cu for semi-hydrogenation of acetylene:Effects of Cu loading [J]. Chinese Journal of Catalysis, 2017, 38(9): 1540-1548.
[13]	Lingyan Wang, Linhai Zhuo, Fengyu Zhao. Carbon dioxide-expanded ethanol-assisted synthesis of carbon-based metal composites and their catalytic and electrochemical performance in lithium-ion batteries [J]. Chinese Journal of Catalysis, 2016, 37(2): 218-226.
[14]	Yu-Lun Fang, Kimberly N. Heck, Zhun Zhao, Lori A. Pretzer, Neng Guo, Tianpin Wu, Jeffrey T. Miller, Michael S. Wong. Gold-doping of carbon-supported palladium improves reduction catalysis [J]. Chinese Journal of Catalysis, 2016, 37(10): 1776-1786.
[15]	Chin-Te Hung, Zih-Hao Liou, Pitchaimani Veerakumar, Pei-Hao Wu, Tuan-Chi Liu, Shang-Bin Liu . Ordered mesoporous carbon supported bifunctional PtM (M = Ru, Fe, Mo) electrocatalysts for a fuel cell anode [J]. Chinese Journal of Catalysis, 2016, 37(1): 43-53.