催化学报

催化学报 ›› 2008, Vol. 29 ›› Issue (1): 86-90.

• 研究论文 • 上一篇    下一篇

非均相温和条件下AlCl3/H2SO4高效催化一锅法合成蒽醌衍生物

Naeimi HOSSEI, Namdari ROOZBEH   

  1. 卡山大学科学学院化学系, 卡山 87317, 伊朗
  • 收稿日期:2008-01-25 出版日期:2008-01-25 发布日期:2011-12-25

Facile, Efficient and One-Pot Synthesis of Anthraquinone Derivatives Catalyzed by AlCl3/H2SO4 under Heterogeneous and Mild Conditions

Naeimi HOSSEI*, Namdari ROOZBEH   

  1. Department of Chemistry, Faculty of Sciences, University of Kashan, Kashan 87317, Iran
  • Received:2008-01-25 Online:2008-01-25 Published:2011-12-25

PDF

782

被引次数

17

摘要： 成功研发了一种与已报道的方法相比合成蒽醌衍生物产量更高的新方法,该方法具有原料易得,收率高,反应时间短,反应条件温和以及操作容易等特点. 合成的蒽醌衍生物的结构由物性数据和光谱结果确定.

关键词: 蒽醌, 路易斯酸, 硫酸, 一锅法合成

Abstract: A new method for the preparation of anthraquinone derivatives with a higher yield than those of previously reported methods was achieved. This method has the advantage of starting with readily available materials. In this reaction the products were obtained in high yield with short reaction time and easy operation under mild conditions. The structure of the products was assigned by physical data and spectroscopic methods.

Key words: anthraquinone, Lewis acid, sulfuric acid, one-pot synthesis